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Title: An Efficient Synthesis of 3-Phosphorylated Benzoxaboroles via the Pudovik Reaction      
dateReleased:
03-18-2017
privacy:
information not avaiable
aggregation:
instance of dataset
dateCreated:
03-18-2017
refinement:
curated
ID:
doi:10.4125/PD0089TH
creators:
Kamath, Prashantha
Rajan, Ramya
Deshpande, Sudhindra
Montgomery, Mark
Lal, Mukul
availability:
available
types:
other
description:
A simple, fast and efficient synthesis of 3-phosphorylated benzoxaboroles using the Pudovik reaction is reported. A number of diverse 3-(dialkoxyphosphoryl)-1-hydroxy-3H-2,1-benzoxaboroles were synthesised in 70–86% yield. Interesting hydrogen bond features were observed in the crystal lattice of the 5-chlorinated 3-bis(benzyl­oxy)phosphoryl derivative with both inter- and intramolecular C–H···O hydrogen bonds. Additionally, linear chains of intermolecular O–H···O hydrogen bonds were observed.
accessURL: https://doi.org/10.4125/PD0089TH
storedIn:
© Georg Thieme Verlag
qualifier:
not compressed
format:
HTML
accessType:
landing page
authentication:
none
authorization:
none
abbreviation:
Thieme Chemistry
homePage: https://www.thieme.de/
ID:
SCR:SCR_014699
name:
Thieme Chemistry

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